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https://doi.org/10.18429/JACoW-SRF2017-TUPB098
Title The Effect of Process Parameters on the Surface Properties of Niobium During Plasma Etching
Authors
  • J.J. Peshl, S. Popović, L. Vušković
    ODU, Norfolk, Virginia, USA
  • J. Upadhyay
    LANL, Los Alamos, New Mexico, USA
  • A-M. Valente-Feliciano
    JLab, Newport News, Virginia, USA
Abstract We have shown that plasma etching using an electronegative Ar/Cl2 discharge can effectively remove surface oxide layers on Nb samples as well as bulk Nb from single cell SRF cavities*. With accelerating fields on the order of wet etching processes and a decrease in field emission the use of plasma assisted etching for bulk Nb processing is a worthwhile endeavor. We are presenting the surface properties of plasma etched Nb. Cavity grade Nb coupons were made by water jet cutting, and then polished to achieve surface roughness equivalent to electropolishing (<1 micron). The coupons were plasma etched while process parameters (rf power, gas pressure, temperature and DC bias voltage) are varied. These samples are placed on the inner surface of the cylindrical cavity to be etched. The experimental setup is similar to the single cell cavity plasma etching setup. Each sample is weighed and scanned before and after plasma processing with an AFM, SEM, and digital optical microscope that provide both atomic composition and surface roughness profiles. Comparing the scans allows us to make conclusions about the effect of each parameter on the surface roughness.
Footnotes & References J. Upadhyay et. al. 'Cryogenic rf test of the first plasma etched SRF cavity,' arXiv: 1605.06494 [physics.acc-ph] (2016).
Funding This work is supported by the Department of Energy, Grant DE-SC0014397.
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Conference SRF2017, Lanzhou, China
Series International Conference on RF Superconductivity (18th)
Proceedings Link to full SRF2017 Proccedings
Session Poster Session
Date 18-Jul-17   14:00–17:00
Main Classification SRF Technology R&D
Sub Classification Cavity processing
Keywords ion, plasma, cavity, experiment, SRF
Publisher JACoW, Geneva, Switzerland
Editors Volker RW Schaa (GSI, Darmstadt, Germany); Yuan He (IMP, Lanzhou, China); Lu Li (IMP, Lanzhou, China); Ning Zhao (IHEP, Beijing, China)
ISBN 978-3-95450-191-5
Published January 2018
Copyright
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cc Creative Commons Attribution 3.0