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https://doi.org/10.18429/JACoW-SRF2017-THPB027
Title Characterization of Microstructural Defects in SRF Cavity Niobium using Electron Channeling Contrast Imaging
Authors
  • M. Wang, T.R. Bieler, D. Kang
    Michigan State University, East Lansing, Michigan, USA
  • C. Compton
    FRIB, East Lansing, Michigan, USA
Abstract Although the quality factor of niobium cavities has improved, performance variability arises from microstructural defects such as dislocations and grain boundaries that can trap magnetic flux, block heat transfer, and perturb superconducting currents. Microstructural defect evolution is compared in four samples extracted from a 2.8 mm thick large-grain niobium slice, with tensile axes chosen to generate desired dislocation structures during deformation. The four samples are 1) as-extracted, 2) extracted and annealed, 3) extracted and then deformed to 40% strain, and 4) extracted, annealed at 800 °C 2 hours, and deformed to 40% strain. Electron Channeling Contrast Imaging (ECCI) was performed on all samples to characterize initial dislocation density, dislocation structure evolution due to annealing and deformation, and related to the mechanical behavior observed in stress-strain curves. The orientation evolution and geometrically necessary dislocation (GND) density were characterized with electron backscattered diffraction (EBSD) maps. Fundamental understanding of dislocation evolution in niobium is necessary to develop models for computational cavity design.
Funding Research supported by DOE/OHEP contract DE-SC0009962
Paper download THPB027.PDF [6.701 MB / 5 pages]
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Conference SRF2017, Lanzhou, China
Series International Conference on RF Superconductivity (18th)
Proceedings Link to full SRF2017 Proccedings
Session Poster Session
Date 20-Jul-17   14:00–17:00
Main Classification Fundamental SRF R&D
Sub Classification Bulk Niobium
Keywords ion, cavity, niobium, electron, SRF
Publisher JACoW, Geneva, Switzerland
Editors Volker RW Schaa (GSI, Darmstadt, Germany); Yuan He (IMP, Lanzhou, China); Lu Li (IMP, Lanzhou, China); Ning Zhao (IHEP, Beijing, China)
ISBN 978-3-95450-191-5
Published January 2018
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