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https://doi.org/10.18429/JACoW-SRF2017-THPB026
Title Investigation of the Effect of Strategically Selected Grain Boundaries on Superconducting Properties of SRF Cavity Niobium
Authors
  • M. Wang, T.R. Bieler
    Michigan State University, East Lansing, Michigan, USA
  • S. Balachandran, P.J. Lee
    NHMFL, Tallahassee, Florida, USA
  • S. Chetri, A. Polyanskii
    ASC, Tallahassee, Florida, USA
  • C. Compton
    FRIB, East Lansing, Michigan, USA
Abstract High purity Nb is commonly used for fabricating SRF cavities due to its high critical temperature and its formability. However, microstructural defects such as dislocations and grain boundaries in niobium can serve as favorable sites for pinning centers of magnetic flux that can degrade SRF cavity performance. In this study, two bi-crystal niobium samples extracted from strategically selected grain boundaries were investigated for the effect of grain misorientation on magnetic flux behavior. Laue X-ray and EBSD-OIM crystallographic analyses were used to characterize grain orientations and orientation gradients. Cryogenic Magneto-Optical Imaging (MOI) was used to directly observe magnetic flux penetration at about 5-8 K. Flux penetration was observed along one of the grain boundaries, as well as along a low angle boundary that was not detected prior to MOI imaging. Hydride scars on the sample surface after MOI were examined using atomic force microscopy (AFM) analysis. The relationships between dislocation content, cryo-cooling, flux penetration and grain boundaries are examined.
Funding Research supported by DOE/OHEP contracts DE-SC0009962, DE-SC0009960, NSF-DMR-1157490, and the State of Florida.
Paper download THPB026.PDF [1.561 MB / 5 pages]
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Conference SRF2017, Lanzhou, China
Series International Conference on RF Superconductivity (18th)
Proceedings Link to full SRF2017 Proccedings
Session Poster Session
Date 20-Jul-17   14:00–17:00
Main Classification Fundamental SRF R&D
Sub Classification Bulk Niobium
Keywords ion, niobium, cavity, SRF, cryogenics
Publisher JACoW, Geneva, Switzerland
Editors Volker RW Schaa (GSI, Darmstadt, Germany); Yuan He (IMP, Lanzhou, China); Lu Li (IMP, Lanzhou, China); Ning Zhao (IHEP, Beijing, China)
ISBN 978-3-95450-191-5
Published January 2018
Copyright
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