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https://doi.org/10.18429/JACoW-LINAC2018-TUPO073
Title Niobium Sample Analysis for Nitrogen Infusion and Doping
Authors
  • T. Konomi, E. Kako, S. Michizono, H. Sakai, K. Umemori
    KEK, Ibaraki, Japan
  • T. Nagata
    ULVAC, Inc., Tsukuba, Japan
  • T. Nojima
    Tohoku University, Sendai, Japan
Abstract KEK has been investigating the better conditions of the heat treatment in nitrogen, which are called as nitrogen doping and nitrogen infusion. We have tried to understand the high gradient performance of the cavity from the analyses of samples which were prepared in the same conditions for the cavity. The main tools are D-SIMS for the depth profile of the elemental concentration, XPS for composition analysis and SQUID magnetometry for the critical DC magnetic field measurement. The difference in the depth profiles of the nitrogen, carbon and oxygen between the heat treatment conditions was observed in vacuum and furnace temperature of nitrogen infusion by D-SIMS and XPS. Such a difference correlates with the vortex penetration field measured by SQUID. In particular, that of nitrogen doping sample was greatly degraded, while that of nitrogen infusion sample was slightly improved. The tendency is similar to the RF high gradient test results. Details of the sample analysis are shown in this presentation.
Paper download TUPO073.PDF [2.098 MB / 4 pages]
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Conference LINAC2018
Series Linear Accelerator Conference (29th)
Location Beijing, China
Date 16-21 September 2018
Publisher JACoW Publishing, Geneva, Switzerland
Editorial Board Guoxi Pei (IHEP, Beijing, China); Volker RW Schaa (GSI, Darmstadt, Germany); Yong Ho Chin (KEK, Tsukuba, Japan); Shinian Fu (IHEP, Beijing, China); Ning Zhao (IHEP, Beijing, China)
Online ISBN 978-3-95450-194-6
Online ISSN 2226-0366
Received 18 September 2018
Accepted 21 September 2018
Issue Date 18 January 2019
DOI doi:10.18429/JACoW-LINAC2018-TUPO073
Copyright
Creative Commons CC logoPublished by JACoW Publishing under the terms of the Creative Commons Attribution 3.0 International license. Any further distribution of this work must maintain attribution to the author(s), the published article's title, publisher, and DOI.